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Beilstein J. Org. Chem. 2019, 15, 1448–1459, doi:10.3762/bjoc.15.145
Graphical Abstract
Scheme 1: The reaction of CDs with oxiranes.
Figure 1: Jar-temperature changes during the reaction of 1,2-propylene oxide and cyclodextrins in the presenc...
Figure 2: Comparative SEM pictures of a β-CD bead and β-CDP (20 mmol, Table 3, entry 10).
Figure 3: Comparison of β-CDP (Table 3, entry 9) and γ-CDP (Table 3, entry 12) prepared in a ball mill on 2 mmol scale.
Figure 4: Normalised particle-size distribution of insoluble CD polymers (entries 9, 10, and 12 of Table 3).
Figure 5: UV–vis spectra and adsorption isotherm of the insoluble β-CDP polymer in 10 ml 0.050 mM MO solution...
Figure 6: UV–vis spectral changes of 0.050 mM MO solution by GPTS-β-CD (left) and GPTS-γ-CD (right), as prepa...
Figure 7: UV–vis spectral changes of 0.050 mM MO solution by GPTS-β-CD (left) and GPTS-γ-CD (right), as prepa...